Crystallography Open Database

Information card for entry 7236022

Preview

Coordinates	7236022.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H34 Cl6 F6 N2 P Sb
Calculated formula	C34 H34 Cl6 F6 N2 P Sb
Title of publication	Hypervalent diorganoantimony(iii) fluorides via diorganoantimony(iii) cations ‒ a general method of synthesis
Authors of publication	Preda, Ana Maria; Raţ, Ciprian I.; Silvestru, Cristian; Lang, Heinrich; Rüffer, Tobias; Mehring, Michael
Journal of publication	RSC Advances
Year of publication	2015
Journal volume	5
Journal issue	121
Pages of publication	99832
a	12.2715 ± 0.0012 Å
b	12.4401 ± 0.0009 Å
c	15.1691 ± 0.001 Å
α	80.778 ± 0.006°
β	71.653 ± 0.008°
γ	70.246 ± 0.008°
Cell volume	2064.9 ± 0.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0698
Residual factor for significantly intense reflections	0.0611
Weighted residual factors for significantly intense reflections	0.1489
Weighted residual factors for all reflections included in the refinement	0.1521
Goodness-of-fit parameter for all reflections included in the refinement	0.973
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
233844 (current)	2019-11-23	cif/ Adding structures of 7236021, 7236022, 7236023, 7236024, 7236025, 7236026 via cif-deposit CGI script.	7236022.cif