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Information card for entry 7238793
Preview
| Coordinates | 7238793.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C37 H34 F24 N4 O P4 |
|---|---|
| Calculated formula | C37 H34 F24 N4 O P4 |
| Title of publication | Rapid and efficient solvent-free synthesis of cyclophanes based on bipyridinium under mechanical ball milling |
| Authors of publication | Xi, Hai-Tao; Zhao, Ting; Sun, Xiao-Qiang; Miao, Chun-Bao; Zong, Ting; Meng, Qi |
| Journal of publication | RSC Adv. |
| Year of publication | 2013 |
| Journal volume | 3 |
| Journal issue | 3 |
| Pages of publication | 691 |
| a | 7.692 ± 0.003 Å |
| b | 20.23 ± 0.007 Å |
| c | 14.097 ± 0.005 Å |
| α | 90° |
| β | 94.13 ± 0.009° |
| γ | 90° |
| Cell volume | 2187.9 ± 1.4 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.2205 |
| Residual factor for significantly intense reflections | 0.0744 |
| Weighted residual factors for significantly intense reflections | 0.1323 |
| Weighted residual factors for all reflections included in the refinement | 0.1699 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.009 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 244355 (current) | 2019-11-28 | cif/ Adding structures of 7238793, 7238794 via cif-deposit CGI script. |
7238793.cif |
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Users of the data should acknowledge the original authors of the
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