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Information card for entry 7238930
Preview
| Coordinates | 7238930.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C15 H29 Cl5 Mo N3 O4 |
|---|---|
| Calculated formula | C15.001 H29 Cl5 Mo N3 O4 |
| Title of publication | Lactam/MoCl5 interaction in CH2Cl2: synthesis and X-ray characterization of protonated δ-valerolactam salts |
| Authors of publication | Marchetti, Fabio; Pampaloni, Guido; Zacchini, Stefano |
| Journal of publication | RSC Advances |
| Year of publication | 2013 |
| Journal volume | 3 |
| Journal issue | 25 |
| Pages of publication | 10007 |
| a | 9.2987 ± 0.0008 Å |
| b | 11.7668 ± 0.001 Å |
| c | 22.2829 ± 0.0018 Å |
| α | 90° |
| β | 101.262 ± 0.001° |
| γ | 90° |
| Cell volume | 2391.2 ± 0.3 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 13 |
| Hermann-Mauguin space group symbol | P 1 2/n 1 |
| Hall space group symbol | -P 2yac |
| Residual factor for all reflections | 0.0285 |
| Residual factor for significantly intense reflections | 0.0234 |
| Weighted residual factors for significantly intense reflections | 0.0531 |
| Weighted residual factors for all reflections included in the refinement | 0.0555 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.02 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 244468 (current) | 2019-11-28 | cif/ Adding structures of 7238929, 7238930 via cif-deposit CGI script. |
7238930.cif |
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Users of the data should acknowledge the original authors of the
structural data.