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Information card for entry 7239024
Preview
| Coordinates | 7239024.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C23 H17 Cl4 Fe O |
|---|---|
| Calculated formula | C23 H17 Cl4 Fe O |
| Title of publication | Selective C‒C bond cleavage of cyclopentadiene rings assisted by ferric chloride to synthesize water-soluble pyrylium salts |
| Authors of publication | Ye, Junwei; Zhang, Xiangdong; Deng, Dai; Ning, Guiling; Liu, Tianqing; Zhuang, Meiling; Yang, Lijian; Gong, Weitao; Lin, Yuan |
| Journal of publication | RSC Advances |
| Year of publication | 2013 |
| Journal volume | 3 |
| Journal issue | 22 |
| Pages of publication | 8232 |
| a | 10.949 ± 0.002 Å |
| b | 17.19 ± 0.003 Å |
| c | 12.099 ± 0.002 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 2277.2 ± 0.7 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 60 |
| Hermann-Mauguin space group symbol | P b c n |
| Hall space group symbol | -P 2n 2ab |
| Residual factor for all reflections | 0.1538 |
| Residual factor for significantly intense reflections | 0.0765 |
| Weighted residual factors for significantly intense reflections | 0.1697 |
| Weighted residual factors for all reflections included in the refinement | 0.2092 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 244512 (current) | 2019-11-28 | cif/ Adding structures of 7239024, 7239025, 7239026, 7239027, 7239028 via cif-deposit CGI script. |
7239024.cif |
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Users of the data should acknowledge the original authors of the
structural data.