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Information card for entry 7239031
Preview
| Coordinates | 7239031.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C28 H20 O |
|---|---|
| Calculated formula | C28 H20 O |
| Title of publication | Synthesis of cyclopentadienyl alkyl ethers via Pd-catalyzed cyclotrimerization of diarylacetylenes |
| Authors of publication | Cai, Ranran; Huang, Mengmeng; Cui, Xiuling; Zhang, Jianye; Du, Chenxia; Wu, Yusheng; Wu, Yangjie |
| Journal of publication | RSC Advances |
| Year of publication | 2013 |
| Journal volume | 3 |
| Journal issue | 32 |
| Pages of publication | 13140 |
| a | 25.7493 ± 0.0014 Å |
| b | 8.1753 ± 0.0003 Å |
| c | 21.7304 ± 0.0012 Å |
| α | 90° |
| β | 117.408 ± 0.007° |
| γ | 90° |
| Cell volume | 4061 ± 0.4 Å3 |
| Cell temperature | 291 ± 2 K |
| Ambient diffraction temperature | 291.15 K |
| Number of distinct elements | 3 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0786 |
| Residual factor for significantly intense reflections | 0.048 |
| Weighted residual factors for significantly intense reflections | 0.1043 |
| Weighted residual factors for all reflections included in the refinement | 0.1209 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.026 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 244514 (current) | 2019-11-28 | cif/ Adding structures of 7239031, 7239032, 7239033 via cif-deposit CGI script. |
7239031.cif |
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Users of the data should acknowledge the original authors of the
structural data.