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Information card for entry 7239096
Preview
Coordinates | 7239096.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C27 H30 S2 |
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Calculated formula | C27 H30 S2 |
Title of publication | A facile synthesis of dithieno[3,2-b:6,7-b]fluorenes via a tandem annulation‒reduction |
Authors of publication | Xiong, Xiaoli; Liu, Qiancai; Zhang, Jun; Zhu, Min; Wang, Yanmei; Deng, Shiming |
Journal of publication | RSC Advances |
Year of publication | 2013 |
Journal volume | 3 |
Journal issue | 39 |
Pages of publication | 17707 |
a | 7.6535 ± 0.0009 Å |
b | 11.5648 ± 0.0014 Å |
c | 13.8466 ± 0.0017 Å |
α | 67.639 ± 0.003° |
β | 84.037 ± 0.004° |
γ | 81.169 ± 0.004° |
Cell volume | 1118.6 ± 0.2 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 3 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0492 |
Residual factor for significantly intense reflections | 0.0357 |
Weighted residual factors for significantly intense reflections | 0.0908 |
Weighted residual factors for all reflections included in the refinement | 0.1006 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.027 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
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244542 (current) | 2019-11-28 | cif/ Adding structures of 7239096 via cif-deposit CGI script. |
7239096.cif |
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Users of the data should acknowledge the original authors of the
structural data.