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Information card for entry 7239266
Preview
| Coordinates | 7239266.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C29 H30 N3 O3 S |
|---|---|
| Calculated formula | C29 H30 N3 O3 S |
| Title of publication | In(OTf)3-catalyzed chemoselective alkylation of tryptamines with 2-oxo-1-pyrrolidine derivatives |
| Authors of publication | Zi, You; Chu, Xue-Qiang; Lu, Xin-Mou; Wang, Shun-Yi; Ji, Shun-Jun |
| Journal of publication | RSC Adv. |
| Year of publication | 2014 |
| Journal volume | 4 |
| Journal issue | 9 |
| Pages of publication | 4609 |
| a | 26.062 ± 0.008 Å |
| b | 15.828 ± 0.005 Å |
| c | 14.693 ± 0.005 Å |
| α | 90° |
| β | 120.379 ± 0.007° |
| γ | 90° |
| Cell volume | 5229 ± 3 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.1594 |
| Residual factor for significantly intense reflections | 0.0871 |
| Weighted residual factors for significantly intense reflections | 0.2303 |
| Weighted residual factors for all reflections included in the refinement | 0.2966 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.075 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 244625 (current) | 2019-11-28 | cif/ Adding structures of 7239265, 7239266 via cif-deposit CGI script. |
7239266.cif |
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Users of the data should acknowledge the original authors of the
structural data.