Crystallography Open Database

Information card for entry 7239282

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Coordinates	7239282.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H16 F N2 O2
Calculated formula	C18 H16 F N2 O2
Title of publication	A green approach for the one-pot multi-component synthesis of N-substituted γ, δ and ε-lactams involving C‒N bond formation catalyzed by FeCl3
Authors of publication	Sathesh, Venkatesan; Sathishkumar, Munusamy; Ramachandran, Gunasekar; Rathore, Ravindranath S.; Sathiyanarayanan, Kulathu Iyer
Journal of publication	RSC Advances
Year of publication	2013
Journal volume	3
Journal issue	45
Pages of publication	23035
a	8.2658 ± 0.0004 Å
b	15.6654 ± 0.0007 Å
c	12.7267 ± 0.0006 Å
α	90°
β	107.505 ± 0.002°
γ	90°
Cell volume	1571.63 ± 0.13 Å³
Cell temperature	295 ± 2 K
Ambient diffraction temperature	295 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0854
Residual factor for significantly intense reflections	0.0588
Weighted residual factors for significantly intense reflections	0.1738
Weighted residual factors for all reflections included in the refinement	0.2014
Goodness-of-fit parameter for all reflections included in the refinement	1.044
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
244634 (current)	2019-11-28	cif/ Adding structures of 7239282 via cif-deposit CGI script.	7239282.cif