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Information card for entry 7239310
Preview
| Coordinates | 7239310.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C30 H0 N O |
|---|---|
| Calculated formula | C30 H26 N O |
| Title of publication | Diastereoselective synthesis of polysubstituted Δ1-pyrroline derivatives from in situ generated nitrile ylides |
| Authors of publication | Guo, Zhi-Wei; Huang, Xiao; Mao, Jia-Min; Zhu, Wei-Dong; Xie, Jian-Wu |
| Journal of publication | RSC Advances |
| Year of publication | 2013 |
| Journal volume | 3 |
| Journal issue | 47 |
| Pages of publication | 25103 |
| a | 9.6811 ± 0.0007 Å |
| b | 14.0805 ± 0.0011 Å |
| c | 18.2882 ± 0.0014 Å |
| α | 67.492 ± 0.004° |
| β | 88.996 ± 0.004° |
| γ | 83.445 ± 0.004° |
| Cell volume | 2287.1 ± 0.3 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.137 |
| Residual factor for significantly intense reflections | 0.0586 |
| Weighted residual factors for significantly intense reflections | 0.1536 |
| Weighted residual factors for all reflections included in the refinement | 0.2011 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.955 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 244647 (current) | 2019-11-28 | cif/ Adding structures of 7239310, 7239311, 7239312, 7239313 via cif-deposit CGI script. |
7239310.cif |
All data in the COD and the database itself are dedicated to the
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.
Users of the data should acknowledge the original authors of the
structural data.