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Information card for entry 7239607
Preview
| Coordinates | 7239607.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C26 H24 O3 S Si2 |
|---|---|
| Calculated formula | C26 H24 O3 S Si2 |
| Title of publication | Sequential cycloaddition and ring expansion reaction of arynes and methylenebenzothiopheneones: synthesis of a benzo-fused eight-membered ring via sulfonium ylides |
| Authors of publication | Xiao, Peng; Su, Shikuan; Wang, Wei; Cao, Weiguo; Chen, Jie; Li, Jian; Chen, Yali |
| Journal of publication | RSC Advances |
| Year of publication | 2019 |
| Journal volume | 9 |
| Journal issue | 67 |
| Pages of publication | 39119 |
| a | 8.38 ± 0.02 Å |
| b | 11.88 ± 0.03 Å |
| c | 13.55 ± 0.04 Å |
| α | 71.08 ± 0.03° |
| β | 78.98 ± 0.03° |
| γ | 75.76 ± 0.03° |
| Cell volume | 1228 ± 6 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0624 |
| Residual factor for significantly intense reflections | 0.0429 |
| Weighted residual factors for significantly intense reflections | 0.1381 |
| Weighted residual factors for all reflections included in the refinement | 0.1739 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.078 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 244826 (current) | 2019-11-30 | cif/ Adding structures of 7239607, 7239608 via cif-deposit CGI script. |
7239607.cif |
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Users of the data should acknowledge the original authors of the
structural data.