Crystallography Open Database

Information card for entry 7239802

Preview

Coordinates	7239802.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H70 K Si3
Calculated formula	C38 H70 K Si3
Title of publication	DMAP-stabilized bis(silyl)silylenes as versatile synthons for organosilicon compounds
Authors of publication	Holzner, Richard; Reiter, Dominik; Frisch, Philipp; Inoue, Shigeyoshi
Journal of publication	RSC Advances
Year of publication	2020
Journal volume	10
Journal issue	6
Pages of publication	3402 - 3406
a	20.678 ± 0.007 Å
b	12.877 ± 0.005 Å
c	17.566 ± 0.01 Å
α	90°
β	120.067 ± 0.01°
γ	90°
Cell volume	4048 ± 3 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0341
Residual factor for significantly intense reflections	0.0305
Weighted residual factors for significantly intense reflections	0.0855
Weighted residual factors for all reflections included in the refinement	0.0886
Goodness-of-fit parameter for all reflections included in the refinement	1.04
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
258055 (current)	2020-10-06	cif/ Updating files of 7239801, 7239802, 7239803, 7239804 Original log message: Adding full bibliography for 7239801--7239804.cif.	7239802.cif
247080	2020-01-22	cif/ Adding structures of 7239801, 7239802, 7239803, 7239804 via cif-deposit CGI script.	7239802.cif