Crystallography Open Database

Information card for entry 7240229

Preview

Coordinates	7240229.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H35 N P2
Calculated formula	C28 H20 N P2
Title of publication	Synthesis of 1,2,4-azadiphosphole derivatives based on vanadium-catalyzed [2+2+1] cycloaddition reactions of azobenzenes with phosphaalkynes
Authors of publication	Liang, Wenbin; Nakajima, Kazunari; Nishibayashi, Yoshiaki
Journal of publication	RSC Advances
Year of publication	2020
Journal volume	10
Journal issue	22
Pages of publication	12730 - 12733
a	14.242 ± 0.0009 Å
b	10.3185 ± 0.0007 Å
c	16.3776 ± 0.0009 Å
α	90°
β	90°
γ	90°
Cell volume	2406.8 ± 0.3 Å³
Cell temperature	178 K
Ambient diffraction temperature	178 K
Number of distinct elements	4
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.1625
Residual factor for significantly intense reflections	0.1398
Weighted residual factors for significantly intense reflections	0.2387
Weighted residual factors for all reflections included in the refinement	0.2519
Goodness-of-fit parameter for all reflections included in the refinement	1
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
257972 (current)	2020-10-06	cif/ Updating files of 7240229 Original log message: Adding full bibliography for 7240229.cif.	7240229.cif
249855	2020-03-31	cif/ Adding structures of 7240229 via cif-deposit CGI script.	7240229.cif