Crystallography Open Database

Information card for entry 7240259

Preview

Coordinates	7240259.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H55 Cu4 N12 O42.5 Si W11
Calculated formula	C12 H48 Cu4 N12 O42.5 Si W11
Title of publication	Application of temperature-controlled chiral hybrid structures constructed from copper(ii)-monosubstituted Keggin polyoxoanions and copper(ii)-organoamine complexes in enantioselective sensing of tartaric acid
Authors of publication	Yang, Mu-Xiu; Zhou, Meng-Jie; Cao, Jia-Peng; Han, Ye-Min; Hong, Ya-Lin; Xu, Yan
Journal of publication	RSC Advances
Year of publication	2020
Journal volume	10
Journal issue	23
Pages of publication	13759 - 13765
a	18.9 ± 0.005 Å
b	23.208 ± 0.006 Å
c	26.175 ± 0.007 Å
α	90°
β	96.397 ± 0.003°
γ	90°
Cell volume	11410 ± 5 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1031
Residual factor for significantly intense reflections	0.0718
Weighted residual factors for significantly intense reflections	0.1717
Weighted residual factors for all reflections included in the refinement	0.1841
Goodness-of-fit parameter for all reflections included in the refinement	1.052
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
258113 (current)	2020-10-06	cif/ Updating files of 7240257, 7240258, 7240259 Original log message: Adding full bibliography for 7240257--7240259.cif.	7240259.cif
250143	2020-04-05	cif/ Adding structures of 7240257, 7240258, 7240259 via cif-deposit CGI script.	7240259.cif