Crystallography Open Database

Information card for entry 7240270

Preview

Coordinates	7240270.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H24 Cl F N2 O3
Calculated formula	C26 H24 Cl F N2 O3
SMILES	Clc1ccc([C@H]2[C@]3(N(C2=O)c2ccc(F)cc2)C(=O)Nc2ccccc32)cc1.O(CC)CC.Clc1ccc([C@@H]2[C@@]3(N(C2=O)c2ccc(F)cc2)C(=O)Nc2ccccc32)cc1.O(CC)CC
Title of publication	Synthesis of 1,3-diaryl-spiro[azetidine-2,3′-indoline]-2′,4-diones via the Staudinger reaction: cis- or trans-diastereoselectivity with different addition modes
Authors of publication	Filatov, Vadim; Kukushkin, Maksim; Kuznetsova, Juliana; Skvortsov, Dmitry; Tafeenko, Viktor; Zyk, Nikolay; Majouga, Alexander; Beloglazkina, Elena
Journal of publication	RSC Advances
Year of publication	2020
Journal volume	10
Journal issue	24
Pages of publication	14122 - 14133
a	14.3504 ± 0.0005 Å
b	9.0371 ± 0.0002 Å
c	20.1515 ± 0.0007 Å
α	90°
β	107.169 ± 0.002°
γ	90°
Cell volume	2496.91 ± 0.14 Å³
Cell temperature	295 ± 2 K
Ambient diffraction temperature	295 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0639
Residual factor for significantly intense reflections	0.0463
Weighted residual factors for significantly intense reflections	0.1338
Weighted residual factors for all reflections included in the refinement	0.1426
Goodness-of-fit parameter for all reflections included in the refinement	1.025
Diffraction radiation wavelength	1.54186 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
257965 (current)	2020-10-06	cif/ Updating files of 7240267, 7240268, 7240269, 7240270, 7240271 Original log message: Adding full bibliography for 7240267--7240271.cif.	7240270.cif
250438	2020-04-07	cif/ Adding structures of 7240267, 7240268, 7240269, 7240270, 7240271 via cif-deposit CGI script.	7240270.cif