Crystallography Open Database

Information card for entry 7241130

Preview

Coordinates	7241130.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22.75 H22 N3 O1.75 S
Calculated formula	C22.75 H22 N3 O1.75 S
Title of publication	Electrochemically enabled synthesis of sulfide imidazopyridines via a radical cyclization cascade
Authors of publication	Zhong, Ping-Fu; Lin, Hong-Min; Wang, Lin-Wei; Mo, Zu-Yu; Meng, Xiu-Jin; Tang, Hai-Tao; Pan, Ying-Ming
Journal of publication	Green Chemistry
Year of publication	2020
Journal volume	22
Journal issue	19
Pages of publication	6334 - 6339
a	4.9241 ± 0.0018 Å
b	14.209 ± 0.004 Å
c	15.299 ± 0.0016 Å
α	90.853 ± 0.015°
β	96.934 ± 0.019°
γ	99.1 ± 0.03°
Cell volume	1048.6 ± 0.5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.2222
Residual factor for significantly intense reflections	0.107
Weighted residual factors for significantly intense reflections	0.2312
Weighted residual factors for all reflections included in the refinement	0.3136
Goodness-of-fit parameter for all reflections included in the refinement	0.89
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
258874 (current)	2020-11-06	cif/ Updating files of 7241129, 7241130, 7241131 Original log message: Adding full bibliography for 7241129--7241131.cif.	7241130.cif
255681	2020-08-27	cif/ Adding structures of 7241129, 7241130, 7241131 via cif-deposit CGI script.	7241130.cif