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Information card for entry 7241662
Preview
| Coordinates | 7241662.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C48 H52 O P2 |
|---|---|
| Calculated formula | C48 H52 O P2 |
| Title of publication | Asymmetric 1,3-dipolar cycloaddition reaction of chiral 1-alkyl-1,2-diphospholes with diphenyldiazomethane |
| Authors of publication | Ganushevich, Yulia; Zagidullin, Almaz; Kondrashova, Svetlana; Latypov, Shamil; Miluykov, Vasili; Lönnecke, Peter; Hey-Hawkins, Evamarie |
| Journal of publication | RSC Advances |
| Year of publication | 2020 |
| Journal volume | 10 |
| Journal issue | 64 |
| Pages of publication | 39060 - 39066 |
| a | 17.2172 ± 0.0004 Å |
| b | 10.339 ± 0.0003 Å |
| c | 22.6719 ± 0.0005 Å |
| α | 90° |
| β | 101.889 ± 0.002° |
| γ | 90° |
| Cell volume | 3949.22 ± 0.17 Å3 |
| Cell temperature | 130 ± 2 K |
| Ambient diffraction temperature | 130 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 5 |
| Hermann-Mauguin space group symbol | C 1 2 1 |
| Hall space group symbol | C 2y |
| Residual factor for all reflections | 0.0745 |
| Residual factor for significantly intense reflections | 0.0524 |
| Weighted residual factors for significantly intense reflections | 0.1224 |
| Weighted residual factors for all reflections included in the refinement | 0.1356 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.006 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 259580 (current) | 2020-12-06 | cif/ Adding structures of 7241662 via cif-deposit CGI script. |
7241662.cif |
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Users of the data should acknowledge the original authors of the
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