Crystallography Open Database

Information card for entry 7241966

7241965 << 7241966 >> 7241967

Preview

Coordinates	7241966.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H16 N16 O7 Rb4 W2
Calculated formula	C32 H16 N16 O7 Rb4 W2
Title of publication	X-ray crystal structures of K+ and Rb+ salts of [W(CN)6(bpy)]2− ion. The unusual cation‒anion interactions and structure changes going from Li+ to Cs+ salts
Authors of publication	Hodorowicz, Maciej; Jurowska, Anna; Szklarzewicz, Janusz
Journal of publication	CrystEngComm
Year of publication	2021
Journal volume	23
Journal issue	5
Pages of publication	1207 - 1217
a	26.6594 ± 0.0003 Å
b	9.2333 ± 0.0001 Å
c	17.6019 ± 0.0002 Å
α	90°
β	93.22 ± 0.001°
γ	90°
Cell volume	4325.94 ± 0.08 Å³
Cell temperature	130 ± 2 K
Ambient diffraction temperature	130 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0592
Residual factor for significantly intense reflections	0.0428
Weighted residual factors for significantly intense reflections	0.0907
Weighted residual factors for all reflections included in the refinement	0.0967
Goodness-of-fit parameter for all reflections included in the refinement	1.05
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
262564 (current)	2021-03-05	cif/ Updating files of 7241966, 7241967 Original log message: Adding full bibliography for 7241966--7241967.cif.	7241966.cif
260131	2020-12-24	cif/ Adding structures of 7241966, 7241967 via cif-deposit CGI script.	7241966.cif