Crystallography Open Database

Information card for entry 7242557

Preview

Coordinates	7242557.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H48 Cl2 N14 Ni2 O8
Calculated formula	C28 H48 Cl2 N14 Ni2 O8
Title of publication	Tuneable structures and magnetic properties of pseudohalo-bridged dinuclear Ni(ii) complexes derived from {N4} and {N3O} donor ligands
Authors of publication	Adak, Sarmistha; Sun, Yu-Chen; Jana, Narayan Ch.; Brandão, Paula; Wang, Xin-Yi; Panja, Anangamohan
Journal of publication	CrystEngComm
Year of publication	2021
Journal volume	23
Journal issue	18
Pages of publication	3371 - 3382
a	8.2434 ± 0.0004 Å
b	13.7798 ± 0.0007 Å
c	16.7261 ± 0.0008 Å
α	90°
β	96.059 ± 0.003°
γ	90°
Cell volume	1889.34 ± 0.16 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0789
Residual factor for significantly intense reflections	0.0452
Weighted residual factors for significantly intense reflections	0.0912
Weighted residual factors for all reflections included in the refinement	0.1054
Goodness-of-fit parameter for all reflections included in the refinement	1.015
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
265985 (current)	2021-06-05	cif/ Updating files of 7242557, 7242558, 7242559, 7242560, 7242561, 7242562 Original log message: Adding full bibliography for 7242557--7242562.cif.	7242557.cif
263424	2021-03-30	cif/ Adding structures of 7242557, 7242558, 7242559, 7242560, 7242561, 7242562 via cif-deposit CGI script.	7242557.cif