Crystallography Open Database

Information card for entry 7242623

Preview

Coordinates	7242623.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C54 H60 Al2 N2 O2
Calculated formula	C54 H60 Al2 N2 O2
Title of publication	Bimetallic aluminum complexes bearing novel spiro-phenanthrene-monoketone/OH derivatives: synthesis, characterization and the ring-opening polymerization of ε-caprolactone
Authors of publication	Yue, Erlin; Cao, Furong; Zhang, Jun; Zhang, Wenjuan; Jiang, Youshu; Liang, Tongling; Sun, Wen-Hua
Journal of publication	RSC Advances
Year of publication	2021
Journal volume	11
Journal issue	22
Pages of publication	13274 - 13281
a	8.9047 ± 0.0018 Å
b	11.867 ± 0.002 Å
c	13.494 ± 0.003 Å
α	94.56 ± 0.03°
β	104.52 ± 0.03°
γ	107.73 ± 0.03°
Cell volume	1295.9 ± 0.6 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0584
Residual factor for significantly intense reflections	0.0504
Weighted residual factors for significantly intense reflections	0.1216
Weighted residual factors for all reflections included in the refinement	0.1261
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
263998 (current)	2021-04-09	cif/ Adding structures of 7242620, 7242621, 7242622, 7242623 via cif-deposit CGI script.	7242623.cif