Crystallography Open Database

Information card for entry 7242636

Preview

Coordinates	7242636.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C210 H178 Cu6 Mo24 N28 O114 Si2
Calculated formula	C210 H180 Cu6 Mo24 N28 O114 Si2
Title of publication	Assembly, structures and properties of polyoxometalate-based supramolecular complexes involving in situ transformation of single-branch N-donor cyano ligands
Authors of publication	Wang, Xiang; Li, Yunhui; Zhang, Tong; Ma, Sijia; Wang, Xiuli
Journal of publication	CrystEngComm
Year of publication	2021
Journal volume	23
Journal issue	19
Pages of publication	3477 - 3487
a	16.2488 ± 0.001 Å
b	19.1465 ± 0.0012 Å
c	24.0881 ± 0.0014 Å
α	67.688 ± 0.001°
β	71.651 ± 0.001°
γ	66.913 ± 0.001°
Cell volume	6255.3 ± 0.7 Å³
Cell temperature	296.15 K
Ambient diffraction temperature	296.15 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1161
Residual factor for significantly intense reflections	0.066
Weighted residual factors for significantly intense reflections	0.1397
Weighted residual factors for all reflections included in the refinement	0.1654
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
265956 (current)	2021-06-05	cif/ Updating files of 7242631, 7242632, 7242633, 7242634, 7242635, 7242636 Original log message: Adding full bibliography for 7242631--7242636.cif.	7242636.cif
264067	2021-04-13	cif/ Adding structures of 7242631, 7242632, 7242633, 7242634, 7242635, 7242636 via cif-deposit CGI script.	7242636.cif