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Information card for entry 7242691
Preview
| Coordinates | 7242691.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C32 H33 N O6 |
|---|---|
| Calculated formula | C32 H33 N O6 |
| Title of publication | Tin(iv) chloride mediated (3 + 2) annulation of trans-2-aroyl-3-styrylcyclopropane-1,1-dicarboxylates with nitriles: diastereoselective access to 5-vinyl-1-pyrroline derivatives |
| Authors of publication | Thangamani, Murugesan; Thangamalar, Subaramaniam; Srinivasan, Kannupal |
| Journal of publication | RSC Advances |
| Year of publication | 2021 |
| Journal volume | 11 |
| Journal issue | 25 |
| Pages of publication | 14980 - 14985 |
| a | 10.0422 ± 0.0006 Å |
| b | 22.1419 ± 0.0014 Å |
| c | 26.2315 ± 0.0015 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 5832.7 ± 0.6 Å3 |
| Cell temperature | 298.08 K |
| Ambient diffraction temperature | 298.08 K |
| Number of distinct elements | 4 |
| Space group number | 61 |
| Hermann-Mauguin space group symbol | P b c a |
| Hall space group symbol | -P 2ac 2ab |
| Residual factor for all reflections | 0.1641 |
| Residual factor for significantly intense reflections | 0.0723 |
| Weighted residual factors for significantly intense reflections | 0.1645 |
| Weighted residual factors for all reflections included in the refinement | 0.2208 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.012 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 264390 (current) | 2021-04-22 | cif/ Adding structures of 7242691 via cif-deposit CGI script. |
7242691.cif |
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Users of the data should acknowledge the original authors of the
structural data.