Crystallography Open Database

Information card for entry 7242922

Preview

Coordinates	7242922.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H23 B Fe Gd N14 O9
Calculated formula	C24 H23 B Fe Gd N14 O9
Title of publication	Cyanido-bridged {FeIIILnIII} heterobimetallic chains assembled through the [FeIII{HB(pz)3}(CN)3]− complex as metalloligand: synthesis, crystal structure and magnetic properties
Authors of publication	Visinescu, Diana; Alexandru, Maria-Gabriela; Dumitrescu, Dan G.; Shova, Sergiu; Moliner, Nicolás; Lloret, Francesc; Julve, Miguel
Journal of publication	CrystEngComm
Year of publication	2021
Journal volume	23
Journal issue	26
Pages of publication	4615 - 4626
a	17.244 ± 0.003 Å
b	14.193 ± 0.003 Å
c	13.216 ± 0.003 Å
α	90°
β	90.93 ± 0.03°
γ	90°
Cell volume	3234.1 ± 1.2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0672
Residual factor for significantly intense reflections	0.0617
Weighted residual factors for significantly intense reflections	0.1673
Weighted residual factors for all reflections included in the refinement	0.171
Goodness-of-fit parameter for all reflections included in the refinement	1.038
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
268662 (current)	2021-09-06	cif/ Updating files of 7242919, 7242920, 7242921, 7242922 Original log message: Adding full bibliography for 7242919--7242922.cif.	7242922.cif
265516	2021-05-27	cif/ Adding structures of 7242919, 7242920, 7242921, 7242922 via cif-deposit CGI script.	7242922.cif