Crystallography Open Database

Information card for entry 7247504

Preview

Coordinates	7247504.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 H50 Cl4 Fe2 N4 P2
Calculated formula	C46 H50 Cl4 Fe2 N4 P2
Title of publication	N-(2-(Diphenylphosphino)ethyl)-2-alkyl-5,6,7,8-tetrahydro-quinolin-8-amines iron(ii) complexes: structural diversity and the ring opening polymerization of ε-caprolactone
Authors of publication	Wang, Yun; Zhang, Wenjuan; Wang, Xing; Zuo, Weiwei; Xue, Xiaopan; Ma, Yanping; Sun, Wen-Hua
Journal of publication	RSC Advances
Year of publication	2023
Journal volume	13
Journal issue	43
Pages of publication	29866 - 29878
a	8.5815 ± 0.0005 Å
b	10.7155 ± 0.0004 Å
c	14.7219 ± 0.0008 Å
α	71.656 ± 0.004°
β	78.877 ± 0.005°
γ	85.997 ± 0.004°
Cell volume	1260.76 ± 0.12 Å³
Cell temperature	169.98 ± 0.11 K
Ambient diffraction temperature	169.98 ± 0.11 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1141
Residual factor for significantly intense reflections	0.1022
Weighted residual factors for significantly intense reflections	0.2587
Weighted residual factors for all reflections included in the refinement	0.2686
Goodness-of-fit parameter for all reflections included in the refinement	1.063
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
286955 (current)	2023-10-13	cif/ Adding structures of 7247504, 7247505, 7247506, 7247507, 7247508, 7247509 via cif-deposit CGI script.	7247504.cif