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Information card for entry 7249395
Preview
| Coordinates | 7249395.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C14 H12 B K N4 O2 |
|---|---|
| Calculated formula | C14 H12 B K N4 O2 |
| Title of publication | Optimised syntheses and purifications of 3-aryl/heterocyclic dihydrobis- and hydrotris-(pyrazolyl)borate ligands as their alkali salts |
| Authors of publication | Thomas, Jarrod R.; Mifsud, Jonathan T.; Sulway, Scott A. |
| Journal of publication | RSC Advances |
| Year of publication | 2024 |
| Journal volume | 14 |
| Journal issue | 42 |
| Pages of publication | 30713 - 30718 |
| a | 11.7918 ± 0.0006 Å |
| b | 23.2058 ± 0.0013 Å |
| c | 5.2271 ± 0.0003 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 1430.33 ± 0.14 Å3 |
| Cell temperature | 100 K |
| Ambient diffraction temperature | 100 K |
| Number of distinct elements | 6 |
| Space group number | 62 |
| Hermann-Mauguin space group symbol | P n m a |
| Hall space group symbol | -P 2ac 2n |
| Residual factor for all reflections | 0.0349 |
| Residual factor for significantly intense reflections | 0.0313 |
| Weighted residual factors for significantly intense reflections | 0.0747 |
| Weighted residual factors for all reflections included in the refinement | 0.0786 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.109 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 294917 (current) | 2024-09-27 | cif/ Adding structures of 7249393, 7249394, 7249395, 7249396, 7249397, 7249398 via cif-deposit CGI script. |
7249395.cif |
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Users of the data should acknowledge the original authors of the
structural data.