Crystallography Open Database

Information card for entry 7249930

Preview

Coordinates	7249930.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H26 Cl N O
Calculated formula	C24 H26 Cl N O
Title of publication	Partial and complete hydrolysis of metal complexes based on monoiminoacenaphthene-1-ones
Authors of publication	Lukoyanov, Anton N.; Zvereva, Yulia V.; Cherkasov, Anton V.; Zhigulin, Grigory Yu.; Kharitonov, Nikita P.; Ketkov, Sergey Yu.
Journal of publication	CrystEngComm
Year of publication	2025
Journal volume	27
Journal issue	12
Pages of publication	1749 - 1762
a	14.4234 ± 0.0007 Å
b	10.4958 ± 0.0004 Å
c	14.8391 ± 0.0007 Å
α	90°
β	110.63 ± 0.005°
γ	90°
Cell volume	2102.37 ± 0.18 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.073
Residual factor for significantly intense reflections	0.0501
Weighted residual factors for significantly intense reflections	0.113
Weighted residual factors for all reflections included in the refinement	0.1259
Goodness-of-fit parameter for all reflections included in the refinement	1.019
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
298871 (current)	2025-04-05	cif/ Updating files of 7249926, 7249927, 7249928, 7249929, 7249930, 7249931, 7249932 Original log message: Adding full bibliography for 7249926--7249932.cif.	7249930.cif
297671	2025-02-11	cif/ Adding structures of 7249926, 7249927, 7249928, 7249929, 7249930, 7249931, 7249932 via cif-deposit CGI script.	7249930.cif