Crystallography Open Database

Information card for entry 7250200

Preview

Coordinates	7250200.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H59 Ni3 O41.5 Rb6
Calculated formula	C30 H52 Ni3 O38 Rb6
Title of publication	The role of alkali metal cations in the construction of heterometallic NiII polymeric cyclopropane-1,1-dicarboxylates
Authors of publication	Zorina-Tikhonova, Ekaterina N.; Matiukhina, Anna K.; Korlyukov, Alexander A.; Goloveshkin, Alexander S.; Babeshkin, Konstantin A.; Efimov, Nikolay N.; Alexandrov, Eugeny V.; Kiskin, Mikhail A.; Eremenko, Igor L.
Journal of publication	CrystEngComm
Year of publication	2025
Journal volume	27
Journal issue	20
Pages of publication	3352 - 3361
a	10.5074 ± 0.0011 Å
b	12.4178 ± 0.0013 Å
c	12.4907 ± 0.0013 Å
α	78.142 ± 0.002°
β	66.982 ± 0.002°
γ	78.702 ± 0.002°
Cell volume	1455.9 ± 0.3 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120.15 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.028
Residual factor for significantly intense reflections	0.021
Weighted residual factors for significantly intense reflections	0.0496
Weighted residual factors for all reflections included in the refinement	0.0517
Goodness-of-fit parameter for all reflections included in the refinement	1.038
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
300716 (current)	2025-07-06	cif/ Updating files of 7250200, 7250201, 7250202, 7250203 Original log message: Adding full bibliography for 7250200--7250203.cif.	7250200.cif
298663	2025-04-01	cif/ Adding structures of 7250200, 7250201, 7250202, 7250203 via cif-deposit CGI script.	7250200.cif