Crystallography Open Database

Information card for entry 7700211

Preview

Coordinates	7700211.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C66 H97 N4 O5 Si2 Sm Zn
Calculated formula	C66 H97 N4 O5 Si2 Sm Zn
Title of publication	Rare-earth/zinc heterometallic complexes containing both alkoxy-amino-bis(phenolato) and chiral salen ligands: synthesis and catalytic application for copolymerization of CO<sub>2</sub> with cyclohexene oxide.
Authors of publication	Xu, Ruoyu; Hua, Linyan; Li, Xiang; Yao, Yingming; Leng, Xuebing; Chen, Yaofeng
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	28
Pages of publication	10565 - 10573
a	10.3825 ± 0.0002 Å
b	26.0638 ± 0.0005 Å
c	15.2519 ± 0.0003 Å
α	90°
β	108.751 ± 0.0009°
γ	90°
Cell volume	3908.22 ± 0.13 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 K
Number of distinct elements	7
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0362
Residual factor for significantly intense reflections	0.0356
Weighted residual factors for significantly intense reflections	0.0959
Weighted residual factors for all reflections included in the refinement	0.0966
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	1.34139 Å
Diffraction radiation type	GaKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
223777 (current)	2019-11-07	cif/ Updating files of 7700208, 7700209, 7700210, 7700211, 7700212 Original log message: Adding full bibliography for 7700208--7700212.cif.	7700211.cif
215772	2019-06-08	cif/ Adding structures of 7700208, 7700209, 7700210, 7700211, 7700212 via cif-deposit CGI script.	7700211.cif