Crystallography Open Database

Information card for entry 7700218

Preview

Coordinates	7700218.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C56 H70 B2 N12 P Se2 Y
Calculated formula	C49 H62 B2 N12 P Se2 Y
Title of publication	Oxidation and chalcogenylative disproportionation of anionic phosphide ligands in yttrium complexes with elemental sulfur and selenium.
Authors of publication	Zhang, Fangjun; Yi, Weiyin; Zhang, Jie; You, Qing; Weng, Linhong; Zhou, Xigeng
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	28
Pages of publication	10596 - 10603
a	14.069 ± 0.004 Å
b	14.446 ± 0.004 Å
c	29.276 ± 0.008 Å
α	90°
β	90.628 ± 0.004°
γ	90°
Cell volume	5950 ± 3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1404
Residual factor for significantly intense reflections	0.0575
Weighted residual factors for significantly intense reflections	0.1056
Weighted residual factors for all reflections included in the refinement	0.1204
Goodness-of-fit parameter for all reflections included in the refinement	1.008
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
223771 (current)	2019-11-07	cif/ Updating files of 7700213, 7700214, 7700215, 7700216, 7700217, 7700218, 7700219, 7700220 Original log message: Adding full bibliography for 7700213--7700220.cif.	7700218.cif
215788	2019-06-09	cif/ Adding structures of 7700213, 7700214, 7700215, 7700216, 7700217, 7700218, 7700219, 7700220 via cif-deposit CGI script.	7700218.cif