Crystallography Open Database

Information card for entry 7700293

Preview

Coordinates	7700293.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C63 H80 Cu2 Gd2 I2 N15 O21
Calculated formula	C63 H80 Cu2 Gd2 I2 N15 O21
Title of publication	Copper(i) iodide cluster-based lanthanide organic frameworks: synthesis and application as efficient catalysts for carboxylative cyclization of propargyl alcohols with CO<sub>2</sub> under mild conditions.
Authors of publication	Wu, Zhilei; Lan, Xingwang; Zhang, Yaxin; Li, Meng; Bai, Guoyi
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	29
Pages of publication	11063 - 11069
a	12.9904 ± 0.0005 Å
b	13.0609 ± 0.0005 Å
c	13.471 ± 0.0006 Å
α	65.919 ± 0.002°
β	86.02 ± 0.002°
γ	82.341 ± 0.002°
Cell volume	2067.76 ± 0.15 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0509
Residual factor for significantly intense reflections	0.0304
Weighted residual factors for significantly intense reflections	0.061
Weighted residual factors for all reflections included in the refinement	0.0679
Goodness-of-fit parameter for all reflections included in the refinement	1.054
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
223759 (current)	2019-11-07	cif/ Updating files of 7700292, 7700293 Original log message: Adding full bibliography for 7700292--7700293.cif.	7700293.cif
216122	2019-06-20	cif/ Adding structures of 7700292, 7700293 via cif-deposit CGI script.	7700293.cif