Crystallography Open Database

Information card for entry 7700296

Preview

Coordinates	7700296.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H57 Cl N6 Si2
Calculated formula	C30 H57 Cl N6 Si2
Title of publication	NHC-stabilized silyl-substituted silyliumylidene ions.
Authors of publication	Frisch, Philipp; Inoue, Shigeyoshi
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	28
Pages of publication	10403 - 10406
a	45.605 ± 0.005 Å
b	45.605 ± 0.005 Å
c	9.2968 ± 0.0011 Å
α	90°
β	90°
γ	120°
Cell volume	16745 ± 3 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	5
Space group number	148
Hermann-Mauguin space group symbol	R -3 :H
Hall space group symbol	-R 3
Residual factor for all reflections	0.0512
Residual factor for significantly intense reflections	0.0432
Weighted residual factors for significantly intense reflections	0.124
Weighted residual factors for all reflections included in the refinement	0.1296
Goodness-of-fit parameter for all reflections included in the refinement	1.104
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
223766 (current)	2019-11-07	cif/ Updating files of 7700296, 7700297 Original log message: Adding full bibliography for 7700296--7700297.cif.	7700296.cif
216124	2019-06-20	cif/ Adding structures of 7700296, 7700297 via cif-deposit CGI script.	7700296.cif