Crystallography Open Database

Information card for entry 7700303

Preview

Coordinates	7700303.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39 H35 Cl3 O0.5 P2 Sb
Calculated formula	C39 H35 Cl3 O0.5 P2 Sb
Title of publication	Hexaphenyl carbodiphosphorane adducts of heavier group 15 element trichlorides: syntheses, properties and reactivities.
Authors of publication	Münzer, Jörn E; Kneusels, Nis-Julian H; Weinert, Bastian; Neumüller, Bernhard; Kuzu, Istemi
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	29
Pages of publication	11076 - 11085
a	10.541 ± 0.001 Å
b	39.489 ± 0.002 Å
c	17.598 ± 0.001 Å
α	90°
β	104.51 ± 0.01°
γ	90°
Cell volume	7091.6 ± 0.9 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0727
Residual factor for significantly intense reflections	0.048
Weighted residual factors for significantly intense reflections	0.0854
Weighted residual factors for all reflections included in the refinement	0.0917
Goodness-of-fit parameter for all reflections included in the refinement	0.891
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
223761 (current)	2019-11-07	cif/ Updating files of 7700302, 7700303, 7700304, 7700305, 7700306, 7700307 Original log message: Adding full bibliography for 7700302--7700307.cif.	7700303.cif
216127	2019-06-20	cif/ Adding structures of 7700302, 7700303, 7700304, 7700305, 7700306, 7700307 via cif-deposit CGI script.	7700303.cif