Crystallography Open Database

Information card for entry 7700747

Preview

Coordinates	7700747.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	[GeCl(N3Dmp2)]
Formula	C50 H55 Cl Ge N3 O0.5
Calculated formula	C50 H55 Cl Ge N3 O0.5
Title of publication	Kinetic stabilization of low-oxidation state and terminal hydrido main group metal complexes by a sterically demanding N,N'-bis(2,6-terphenyl)triazenide.
Authors of publication	Leverett, Anthony R.; Diachenko, Vera; Cole, Marcus L.; McKay, Alasdair I.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	35
Pages of publication	13197 - 13204
a	10.637 ± 0.014 Å
b	11.483 ± 0.015 Å
c	20.41 ± 0.03 Å
α	102.8 ± 0.04°
β	94.73 ± 0.03°
γ	111.41 ± 0.04°
Cell volume	2226 ± 5 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1764
Residual factor for significantly intense reflections	0.0892
Weighted residual factors for significantly intense reflections	0.2165
Weighted residual factors for all reflections included in the refinement	0.2772
Goodness-of-fit parameter for all reflections included in the refinement	1.039
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
224492 (current)	2019-11-08	cif/ Updating files of 7700747, 7700748, 7700749, 7700750, 7700751, 7700752, 7700753, 7700754, 7700755, 7700756, 7700757, 7700758, 7700759, 7700760, 7700761 Original log message: Adding full bibliography for 7700747--7700761.cif.	7700747.cif
217447	2019-08-07	cif/ Adding structures of 7700747, 7700748, 7700749, 7700750, 7700751, 7700752, 7700753, 7700754, 7700755, 7700756, 7700757, 7700758, 7700759, 7700760, 7700761 via cif-deposit CGI script.	7700747.cif