Crystallography Open Database

Information card for entry 7700852

Preview

Coordinates	7700852.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H45 Cl7 N2 O3 P2 Ru
Calculated formula	C52 H45 Cl7 N2 O3 P2 Ru
Title of publication	Unusual C-O bond cleavage of aromatic ethers in ruthenium complexes bearing a 2-alkoxypyridyl fragment.
Authors of publication	Deng, Danfeng; Hu, Bowen; Yang, Min; Chen, Dafa
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	36
Pages of publication	13614 - 13621
a	11.8566 ± 0.0005 Å
b	14.881 ± 0.0005 Å
c	15.3961 ± 0.0005 Å
α	83.417 ± 0.003°
β	87.037 ± 0.003°
γ	74.939 ± 0.003°
Cell volume	2605.17 ± 0.17 Å³
Cell temperature	173 ± 0.1 K
Ambient diffraction temperature	173 ± 0.1 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0975
Residual factor for significantly intense reflections	0.0746
Weighted residual factors for significantly intense reflections	0.2049
Weighted residual factors for all reflections included in the refinement	0.227
Goodness-of-fit parameter for all reflections included in the refinement	1.056
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
224470 (current)	2019-11-08	cif/ Updating files of 7700852, 7700853, 7700854, 7700855 Original log message: Adding full bibliography for 7700852--7700855.cif.	7700852.cif
217568	2019-08-17	cif/ Adding structures of 7700852, 7700853, 7700854, 7700855 via cif-deposit CGI script.	7700852.cif