Crystallography Open Database

Information card for entry 7701325

Preview

Coordinates	7701325.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C9 H26 B11 Cu N2
Calculated formula	C9 H26 B11 Cu N2
Title of publication	The 12-ethynylmonocarba-closo-dodecaborate anion as a versatile ligand for Cu(I) alkyne and heterobimetallic Cu(I)/M(II) (M = Pd, Pt) alkynide complexes
Authors of publication	Jiang, Tao; Zhang, Kang; Shen, Yunjun; Hamdaoui, Mustapha; Dontha, Rakesh; Liu, Jiyong; Spingler, Bernhard; Duttwyler, Simon
Journal of publication	Dalton Transactions
Year of publication	2019
a	27.1076 ± 0.0007 Å
b	7.1263 ± 0.0002 Å
c	19.486 ± 0.0005 Å
α	90°
β	102.529 ± 0.002°
γ	90°
Cell volume	3674.6 ± 0.17 Å³
Cell temperature	170 ± 2 K
Ambient diffraction temperature	170 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.094
Residual factor for significantly intense reflections	0.0485
Weighted residual factors for significantly intense reflections	0.0841
Weighted residual factors for all reflections included in the refinement	0.1006
Goodness-of-fit parameter for all reflections included in the refinement	1.013
Diffraction radiation wavelength	1.34139 Å
Diffraction radiation type	GaKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
219231 (current)	2019-10-10	cif/ Adding structures of 7701325, 7701326, 7701327, 7701328, 7701329, 7701330, 7701331, 7701332, 7701333, 7701334 via cif-deposit CGI script.	7701325.cif