Crystallography Open Database

Information card for entry 7701467

Preview

Coordinates	7701467.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	18145zz
Chemical name	W(CO)3{h6-(((3,5-CH3)C6H3)BPPh3)Cr(CO)3}
Formula	C53 H45 B Cr O6 P3 W
Calculated formula	C53 H45 B Cr O6 P3 W
Title of publication	Seventeen-electron chromium(i)tricarbonyltris(phosphine) complexes supported by tris(phosphinomethyl)phenylborates
Authors of publication	Fischer, Paul J.; Senthil, Shuruthi; Stephan, Jeremy T.; Swift, McKinley L.; Young, Victor G.
Journal of publication	Dalton Transactions
Year of publication	2019
a	13.198 ± 0.003 Å
b	13.261 ± 0.003 Å
c	17.397 ± 0.004 Å
α	78.336 ± 0.004°
β	78.808 ± 0.004°
γ	61.407 ± 0.004°
Cell volume	2601.4 ± 1 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0484
Residual factor for significantly intense reflections	0.0365
Weighted residual factors for significantly intense reflections	0.0828
Weighted residual factors for all reflections included in the refinement	0.0903
Goodness-of-fit parameter for all reflections included in the refinement	1.087
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
220619 (current)	2019-11-01	cif/ Adding structures of 7701464, 7701465, 7701466, 7701467, 7701468, 7701469, 7701470 via cif-deposit CGI script.	7701467.cif