Crystallography Open Database

Information card for entry 7701672

Preview

Coordinates	7701672.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H40 Cu1.5 F36 N8 O16 Tb
Calculated formula	C52 H40 Cu1.5 F36 N8 O16 Tb
Title of publication	Synthesis of a series of hetero-multi-spin Ln<sub>2</sub>Cu<sub>3</sub> complexes based on a methyl-pyrazole nitronyl nitroxide radical with slow magnetic relaxation behaviors.
Authors of publication	Shi, Jian Yun; Chen, Peng Yun; Wu, Ming Ze; Tian, Li; Liu, Zhong Yi
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	25
Pages of publication	9187 - 9193
a	11.9225 ± 0.0002 Å
b	18.33 ± 0.0003 Å
c	20.3485 ± 0.0004 Å
α	94.5361 ± 0.0015°
β	92.497 ± 0.0015°
γ	95.6302 ± 0.0015°
Cell volume	4405.73 ± 0.14 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0465
Residual factor for significantly intense reflections	0.0439
Weighted residual factors for significantly intense reflections	0.1123
Weighted residual factors for all reflections included in the refinement	0.1146
Goodness-of-fit parameter for all reflections included in the refinement	1.023
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
223331 (current)	2019-11-05	cif/ Adding structures of 7701672, 7701673, 7701674 via cif-deposit CGI script.	7701672.cif