Crystallography Open Database

Information card for entry 7701683

Preview

Coordinates	7701683.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C53 H64 As2 Cl4 N2 O Zr
Calculated formula	C53 H64 As2 Cl4 N2 O Zr
Title of publication	Synthesis and structural characterization of arsinoamides - early transition metal (Zr and Hf) and main group metal (Al, In, Sn, and Pb) complexes.
Authors of publication	Chen, Xiao; Gamer, Michael T.; Roesky, Peter W.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	40
Pages of publication	15207 - 15211
a	12.3693 ± 0.0006 Å
b	16.8828 ± 0.0005 Å
c	25.026 ± 0.0011 Å
α	90°
β	102.369 ± 0.004°
γ	90°
Cell volume	5104.8 ± 0.4 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1011
Residual factor for significantly intense reflections	0.0523
Weighted residual factors for significantly intense reflections	0.1107
Weighted residual factors for all reflections included in the refinement	0.1305
Goodness-of-fit parameter for all reflections included in the refinement	1.012
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
223335 (current)	2019-11-05	cif/ Adding structures of 7701683, 7701684, 7701685, 7701686, 7701687, 7701688, 7701689, 7701690 via cif-deposit CGI script.	7701683.cif