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Information card for entry 7701894
Preview
| Coordinates | 7701894.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C44 H44 Ni O P2 S2 |
|---|---|
| Calculated formula | C44 H44 Ni O P2 S2 |
| Title of publication | Reactivity of the diphosphinodithio ligated nickel(0) complex toward alkyl halides and resultant nickel(i) and nickel(ii)-alkyl complexes. |
| Authors of publication | Zhang, Ailing; Wang, Congxiao; Lai, Xiaoyu; Zhai, Xiaofang; Pang, Maofu; Tung, Chen-Ho; Wang, Wenguang |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2018 |
| Journal volume | 47 |
| Journal issue | 44 |
| Pages of publication | 15757 - 15764 |
| a | 9.5713 ± 0.0003 Å |
| b | 13.7242 ± 0.0005 Å |
| c | 14.7211 ± 0.0003 Å |
| α | 85.898 ± 0.002° |
| β | 86.077 ± 0.002° |
| γ | 80.81 ± 0.003° |
| Cell volume | 1900.84 ± 0.1 Å3 |
| Cell temperature | 173 ± 0.1 K |
| Ambient diffraction temperature | 173 ± 0.1 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0459 |
| Residual factor for significantly intense reflections | 0.0344 |
| Weighted residual factors for significantly intense reflections | 0.0841 |
| Weighted residual factors for all reflections included in the refinement | 0.0908 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.067 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 227798 (current) | 2019-11-14 | cif/ Adding structures of 7701894, 7701895, 7701896 via cif-deposit CGI script. |
7701894.cif |
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Users of the data should acknowledge the original authors of the
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