Crystallography Open Database

Information card for entry 7701992

7701991 << 7701992 >> 7701993

Preview

Coordinates	7701992.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C43 H52 Cl2 F3 N2 Ni O3 P S Si
Calculated formula	C43 H52 Cl2 F3 N2 Ni O3 P S Si
Title of publication	Neutral, cationic and anionic organonickel and -palladium complexes supported by iminophosphine/phosphinoenaminato ligands.
Authors of publication	Santiago, Tomás G; Urbaneja, Carmen; Álvarez, Eleuterio; Ávila, Elena; Palma, Pilar; Cámpora, Juan
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	2
Pages of publication	322 - 335
a	10.8549 ± 0.0005 Å
b	12.204 ± 0.0006 Å
c	18.5076 ± 0.0009 Å
α	96.275 ± 0.002°
β	94.927 ± 0.002°
γ	94.771 ± 0.002°
Cell volume	2417.4 ± 0.2 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	10
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0591
Residual factor for significantly intense reflections	0.0426
Weighted residual factors for significantly intense reflections	0.1171
Weighted residual factors for all reflections included in the refinement	0.1268
Goodness-of-fit parameter for all reflections included in the refinement	1.057
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
247733 (current)	2020-02-04	cif/ Updating files of 7701989, 7701990, 7701991, 7701992, 7701993 Original log message: Adding full bibliography for 7701989--7701993.cif.	7701992.cif
231109	2019-11-21	cif/ Adding structures of 7701989, 7701990, 7701991, 7701992, 7701993 via cif-deposit CGI script.	7701992.cif