Crystallography Open Database

Information card for entry 7702054

7702053 << 7702054 >> 7702055

Preview

Coordinates	7702054.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C45 H54 Cd Cl2 N6 O10 Se3
Calculated formula	C45 H54 Cd Cl2 N6 O10 Se3
Title of publication	Facile access to zinc and cadmium selones: highly active catalysts for Barbier reactions in aqueous media.
Authors of publication	Naga Babu, Chatla; Srinivas, Katam; Prabusankar, Ganesan
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	15
Pages of publication	6456 - 6465
a	14.618 ± 0.0003 Å
b	14.618 ± 0.0003 Å
c	45.0966 ± 0.001 Å
α	90°
β	90°
γ	120°
Cell volume	8345.5 ± 0.3 Å³
Cell temperature	293 K
Ambient diffraction temperature	293 K
Number of distinct elements	7
Space group number	148
Hermann-Mauguin space group symbol	R -3 :H
Hall space group symbol	-R 3
Residual factor for all reflections	0.045
Residual factor for significantly intense reflections	0.0417
Weighted residual factors for significantly intense reflections	0.1416
Weighted residual factors for all reflections included in the refinement	0.1482
Goodness-of-fit parameter for all reflections included in the refinement	1.0384
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
233452 (current)	2019-11-23	cif/ Adding structures of 7702050, 7702051, 7702052, 7702053, 7702054, 7702055, 7702056 via cif-deposit CGI script.	7702054.cif