Crystallography Open Database

Information card for entry 7702283

Preview

Coordinates	7702283.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C64 H84 Cl8 Mg4 N4 O14
Calculated formula	C64 H83.996 Cl8 Mg4 N4 O13.999
Title of publication	Syntheses, structures and catalytic activity of tetranuclear Mg complexes in the ROP of cyclic esters under industrially relevant conditions.
Authors of publication	Ghosh, Swarup; Wölper, Christoph; Tjaberings, Alexander; Gröschel, André H; Schulz, Stephan
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	2
Pages of publication	375 - 387
a	15.6933 ± 0.0009 Å
b	15.6933 ± 0.0009 Å
c	28.4979 ± 0.0019 Å
α	90°
β	90°
γ	90°
Cell volume	7018.5 ± 0.7 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	78
Hermann-Mauguin space group symbol	P 43
Hall space group symbol	P 4cw
Residual factor for all reflections	0.0709
Residual factor for significantly intense reflections	0.0488
Weighted residual factors for significantly intense reflections	0.1132
Weighted residual factors for all reflections included in the refinement	0.1262
Goodness-of-fit parameter for all reflections included in the refinement	1.027
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
247727 (current)	2020-02-04	cif/ Updating files of 7702280, 7702281, 7702282, 7702283 Original log message: Adding full bibliography for 7702280--7702283.cif.	7702283.cif
243806	2019-11-28	cif/ Adding structures of 7702280, 7702281, 7702282, 7702283 via cif-deposit CGI script.	7702283.cif