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Information card for entry 7702411
Preview
| Coordinates | 7702411.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C21 H27 B N9 O2 Re S Si |
|---|---|
| Calculated formula | C21 H27 B N9 O2 Re S Si |
| Title of publication | Control of the hapticity of pyridine-2-thiolate ligands in rhenium(V) oxo complexes † |
| Authors of publication | Paulo, António; Domingos, Ângela; Santos, Isabel |
| Journal of publication | Journal of the Chemical Society, Dalton Transactions |
| Year of publication | 1999 |
| Journal issue | 21 |
| Pages of publication | 3735 |
| a | 17.545 ± 0.003 Å |
| b | 8.2966 ± 0.0009 Å |
| c | 19.997 ± 0.003 Å |
| α | 90° |
| β | 110.91 ± 0.01° |
| γ | 90° |
| Cell volume | 2719.1 ± 0.7 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 8 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.1369 |
| Residual factor for significantly intense reflections | 0.075 |
| Weighted residual factors for all reflections | 0.1892 |
| Weighted residual factors for significantly intense reflections | 0.1358 |
| Goodness-of-fit parameter for all reflections | 1.113 |
| Goodness-of-fit parameter for significantly intense reflections | 1.088 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 243858 (current) | 2019-11-28 | cif/ Adding structures of 7702411, 7702412, 7702413 via cif-deposit CGI script. |
7702411.cif |
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Users of the data should acknowledge the original authors of the
structural data.