Crystallography Open Database

Information card for entry 7702427

Preview

Coordinates	7702427.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	[Li2(thf){Me3SiNCHNCHNCH(SiMe3)2}2]
Formula	C30 H68 Li2 N6 O Si6
Calculated formula	C30 H68 Li2 N6 O Si6
Title of publication	Reactions of 1,3,5-triazine with organolithium compounds containing trimethylsilyl substituents; X-ray structures of 1,3,5-triaza- and 1,3,5,7-tetraaza-heptatrienyllithium compounds †
Authors of publication	Boesveld, W. Marco; Hitchcock, Peter B.; Lappert, Michael F.
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	1999
Journal issue	22
Pages of publication	4041
a	13.022 ± 0.003 Å
b	8.134 ± 0.004 Å
c	22.607 ± 0.006 Å
α	90°
β	106.43 ± 0.02°
γ	90°
Cell volume	2296.8 ± 1.4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/n 1
Hall space group symbol	-P 2yac
Residual factor for all reflections	0.1112
Residual factor for significantly intense reflections	0.0621
Weighted residual factors for all reflections	0.1615
Weighted residual factors for significantly intense reflections	0.1361
Goodness-of-fit parameter for all reflections	1.044
Goodness-of-fit parameter for significantly intense reflections	1.114
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
243861 (current)	2019-11-28	cif/ Adding structures of 7702426, 7702427, 7702428, 7702429 via cif-deposit CGI script.	7702427.cif