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Information card for entry 7702435
Preview
| Coordinates | 7702435.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C26 H30 I6 N4 S2 |
|---|---|
| Calculated formula | C26 H30 I6 N4 S2 |
| Title of publication | Conversion of some substituted phenols to the corresponding masked thiophenols, synthesis of a dinickel(II) dithiolate macrocyclic complex and isolation of some metal- and ligand-based oxidation products |
| Authors of publication | Brooker, Sally; Caygill, Graham B.; Croucher, Paul D.; Davidson, Tony C.; Clive, Derrick L. J.; Magnuson, Stephen R.; Cramer, Stephen P.; Ralston, Corie Y. |
| Journal of publication | Journal of the Chemical Society, Dalton Transactions |
| Year of publication | 2000 |
| Journal issue | 18 |
| Pages of publication | 3113 |
| a | 8.9104 ± 0.0019 Å |
| b | 9.1521 ± 0.0019 Å |
| c | 12.172 ± 0.003 Å |
| α | 70.605 ± 0.003° |
| β | 85.336 ± 0.003° |
| γ | 68.074 ± 0.003° |
| Cell volume | 867.5 ± 0.3 Å3 |
| Cell temperature | 168 ± 2 K |
| Ambient diffraction temperature | 168 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0346 |
| Residual factor for significantly intense reflections | 0.0284 |
| Weighted residual factors for significantly intense reflections | 0.0692 |
| Weighted residual factors for all reflections included in the refinement | 0.0715 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.093 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 243866 (current) | 2019-11-28 | cif/ Adding structures of 7702433, 7702434, 7702435, 7702436, 7702437 via cif-deposit CGI script. |
7702435.cif |
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Users of the data should acknowledge the original authors of the
structural data.