Crystallography Open Database

Information card for entry 7702480

Preview

Coordinates	7702480.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C75 H89 Cl2 Cu N4 O3.5 P2
Calculated formula	C74.5 H62 Cl2 Cu N4 O3.5 P2
Title of publication	Synthesis and characterization of bulky salen-type complexes of Co, Cu, Fe, Mn and Ni with amphiphilic solubility properties
Authors of publication	Haikarainen, Anssi; Sipilä, Jussi; Pietikäinen, Pekka; Pajunen, Aarne; Mutikainen, Ilpo
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2001
Journal issue	7
Pages of publication	991
a	14.941 ± 0.008 Å
b	19.023 ± 0.008 Å
c	13.869 ± 0.006 Å
α	95.42 ± 0.05°
β	116.06 ± 0.05°
γ	88.96 ± 0.05°
Cell volume	3524 ± 3 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1335
Residual factor for significantly intense reflections	0.11
Weighted residual factors for all reflections	0.3347
Weighted residual factors for significantly intense reflections	0.308
Weighted residual factors for all reflections included in the refinement	0.3347
Goodness-of-fit parameter for all reflections	1.336
Goodness-of-fit parameter for all reflections included in the refinement	1.336
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
243877 (current)	2019-11-28	cif/ Adding structures of 7702480, 7702481 via cif-deposit CGI script.	7702480.cif