Crystallography Open Database

Information card for entry 7702482

Preview

Coordinates	7702482.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Triphenylphosphine chloro 2(N,N-dimethylamino)ethylselenolato palladium(II)
Formula	C22 H25 Cl N P Pd Se
Calculated formula	C22 H25 Cl N P Pd Se
Title of publication	2-(Dimethylamino)ethaneselenolates of palladium(II): synthesis, structure, spectroscopy and transformation into palladium selenide
Authors of publication	Dey, Sandip; Jain, Vimal K.; Chaudhury, Satyajeet; Knoedler, Axel; Lissner, Falk; Kaim, Wolfgang
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2001
Journal issue	5
Pages of publication	723
a	9.5268 ± 0.0019 Å
b	19.827 ± 0.004 Å
c	11.661 ± 0.002 Å
α	90°
β	95.77 ± 0.03°
γ	90°
Cell volume	2191.5 ± 0.7 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0597
Residual factor for significantly intense reflections	0.0478
Weighted residual factors for significantly intense reflections	0.1354
Weighted residual factors for all reflections included in the refinement	0.1469
Goodness-of-fit parameter for all reflections included in the refinement	1.086
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
243878 (current)	2019-11-28	cif/ Adding structures of 7702482, 7702483 via cif-deposit CGI script.	7702482.cif