Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7702574
Preview
| Coordinates | 7702574.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C75 H78 Nb O2 Si3 |
|---|---|
| Calculated formula | C75 H78 Nb O2 Si3 |
| Title of publication | Studies of the alkylation of niobium and tantalum halides containing 2,6-diarylphenoxide ancillary ligation |
| Authors of publication | Schweiger, Scott W.; Salberg, Michelle M.; Pulvirenti, April L.; Freeman, Emily E.; Fanwick, Phillip E.; Rothwell, Ian P. |
| Journal of publication | Journal of the Chemical Society, Dalton Transactions |
| Year of publication | 2001 |
| Journal issue | 13 |
| Pages of publication | 2020 |
| a | 12.762 ± 0.0003 Å |
| b | 18.0027 ± 0.0004 Å |
| c | 28.8284 ± 0.0007 Å |
| α | 90° |
| β | 95.5229 ± 0.0014° |
| γ | 90° |
| Cell volume | 6592.6 ± 0.3 Å3 |
| Cell temperature | 203 K |
| Ambient diffraction temperature | 203 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for significantly intense reflections | 0.049 |
| Weighted residual factors for all reflections included in the refinement | 0.11 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.033 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MO-Kα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 243909 (current) | 2019-11-28 | cif/ Adding structures of 7702564, 7702565, 7702566, 7702567, 7702568, 7702569, 7702570, 7702571, 7702572, 7702573, 7702574, 7702575, 7702576, 7702577 via cif-deposit CGI script. |
7702574.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.