Crystallography Open Database

Information card for entry 7702603

Preview

Coordinates	7702603.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H36 Mo O18 Re3
Calculated formula	C12 H36 Mo0.993333 O17.8 Re3.014
Title of publication	Homo- and hetero-metallic rhenium oxomethoxide complexes with a M4(µ-O)2(µ-OMe)4 planar core—a new family of metal alkoxides displaying a peculiar structural disorder. Preparation and X-ray single crystal study
Authors of publication	Seisenbaeva, Gulaim A.; Shevelkov, Andrei V.; Tegenfeldt, Jörgen; Kloo, Lars; Drobot, Dmitrii V.; Kessler, Vadim G.
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2001
Journal issue	19
Pages of publication	2762
a	7.9141 ± 0.0004 Å
b	16.0535 ± 0.0008 Å
c	17.5938 ± 0.0009 Å
α	113.322 ± 0.001°
β	93.355 ± 0.001°
γ	92.754 ± 0.001°
Cell volume	2042.93 ± 0.18 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0953
Residual factor for significantly intense reflections	0.0685
Weighted residual factors for significantly intense reflections	0.1575
Weighted residual factors for all reflections included in the refinement	0.1632
Goodness-of-fit parameter for all reflections included in the refinement	0.897
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
243921 (current)	2019-11-28	cif/ Adding structures of 7702602, 7702603, 7702604, 7702605, 7702606 via cif-deposit CGI script.	7702603.cif