Crystallography Open Database

Information card for entry 7702605

Preview

Coordinates	7702605.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C14 H42 Nb4 O24 Re2
Calculated formula	C14 H42 Nb4 O24 Re2
Title of publication	Homo- and hetero-metallic rhenium oxomethoxide complexes with a M4(µ-O)2(µ-OMe)4 planar core—a new family of metal alkoxides displaying a peculiar structural disorder. Preparation and X-ray single crystal study
Authors of publication	Seisenbaeva, Gulaim A.; Shevelkov, Andrei V.; Tegenfeldt, Jörgen; Kloo, Lars; Drobot, Dmitrii V.; Kessler, Vadim G.
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2001
Journal issue	19
Pages of publication	2762
a	9.716 ± 0.004 Å
b	15.888 ± 0.007 Å
c	12.128 ± 0.006 Å
α	90°
β	101.059 ± 0.009°
γ	90°
Cell volume	1837.4 ± 1.4 Å³
Cell temperature	295 ± 2 K
Ambient diffraction temperature	295 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1016
Residual factor for significantly intense reflections	0.0552
Weighted residual factors for significantly intense reflections	0.1422
Weighted residual factors for all reflections included in the refinement	0.1564
Goodness-of-fit parameter for all reflections included in the refinement	0.875
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
243921 (current)	2019-11-28	cif/ Adding structures of 7702602, 7702603, 7702604, 7702605, 7702606 via cif-deposit CGI script.	7702605.cif