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Information card for entry 7702663
Preview
| Coordinates | 7702663.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C38 H41 F6 Ir O3 P2 |
|---|---|
| Calculated formula | C38 H41 F6 Ir O3 P2 |
| Title of publication | Novel single or double insertion of alkynes into rhodium‒ and iridium‒oxygen or ‒phosphorus atom bonds and transannular addition of 1-alkynes between the rhodium atom and the ipso-carbon atom of the phosphorus ligand |
| Authors of publication | Yamamoto, Yasuhiro; Sugawara, Kenichiro; Han, Xiao-Hong |
| Journal of publication | Journal of the Chemical Society, Dalton Transactions |
| Year of publication | 2002 |
| Journal issue | 2 |
| Pages of publication | 195 |
| a | 15.06 ± 0.009 Å |
| b | 13.36 ± 0.008 Å |
| c | 18.705 ± 0.009 Å |
| α | 90° |
| β | 90.84 ± 0.04° |
| γ | 90° |
| Cell volume | 3763 ± 4 Å3 |
| Cell temperature | 300.2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for significantly intense reflections | 0.0441 |
| Weighted residual factors for all reflections included in the refinement | 0.1213 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.978 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 243940 (current) | 2019-11-28 | cif/ Adding structures of 7702656, 7702657, 7702658, 7702659, 7702660, 7702661, 7702662, 7702663, 7702664, 7702665, 7702666 via cif-deposit CGI script. |
7702663.cif |
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Users of the data should acknowledge the original authors of the
structural data.